SummaryThedeterminationoftheamountofoxygen,nitrogen,andhydrogeniniron,steel,nickel-,andcobalt-basealloysrepresentssomeofthemostimportantqualitymetricsforthesematerials.Oxygenisusedtocreatesteelfrompigironbyremovingexcesscarbon.Oxygencontentmustbecontrolledtolimittheamountofcarbonmonoxidethatcanbeformedduringsolidificationwhichmaycauseexcessiveporosity.Nitrogenisconsideredbothanimpurityaswellasanimportantalloyingagent.Itcanbepresentasanitrideorinterstitiallyinitsgaseousform.Increasednitrogencontentisknowntoincreaseyieldandtensilestrength,thusdecreasingductilityandformability.Excessivelevelsmayevolveduringsolidificationthusincreasingporosity.Highhydrogencontentistheprimarycauseofembrittlement,blisteringandflakingduetoitshighmobilitythroughthelatticeandprovidesnopotentialalloyingbenefits.TheONH836utilizesahigh-powerelectrodefurnacetoquicklyandefficientlyreleasethetargetgasesfromwithinthesample,whichallowsforaveryrapidsimultaneousdeterminationofoxygen,nitrogen,andhydrogen.分析仪,就选上海禹重实业有限公司。淮安LECO分析仪
MethodSelectionTwomethodsaredescribedinthisapplicationnote;eithermethodcanbeusedtoanalyzeiron,steel,nickel-,andcobalt-basealloys.ThePrecisionMethodisrecommendedforgeneraluseandwillprovidethebestprecisionandaccuracythroughoutthetypicalO,N,andHconcentrationsfoundinthisgroupofmetals;approximatecycletimeis3.5minutes.TheFastTrackmethodcanbeusedwherespeedofanalysisisacriticalcomponent;forexample,whenmoltenmetalisbeingsampledandresultsarerequiredintheshortestpossibletime.Thismethodwillproducesuitableresultsformostsamples;approximatecycletimeis2.25minutes.Asnotedabove,samplingandsamplepreparationarekeyelementstoaccurateO,N,andHdeterminationaswell.Itisuptotheusertodeterminewhichmethodbestmeetstheirneeds.淮安LECO分析仪上海禹重实业有限公司为您提供分析仪,期待为您服务!
Procedure–Powder/ChipSamplesInstrumentcalibration/driftcorrection.Calibrate/driftfollowingtheprocedureoutlinedintheoperatorsinstructionmanual.AnalyzeSamples.LoginSamplewiththeappropriatenumberofreps.Weighapproximately***gramsofappropriatelypreparedsampleintoa***NickelCapsule,entermassandsampleidentificationintoappropriaterepfields.Ifapplicable,placethenickelcapsuleintheappropriateautoloaderposition.Repeatsteps3cthrough3iforsampleanalysis.
Procedure-SolidSamplesDeterminetheinstrumentblank.Repeatsteps2bthrough2gaminimumofthreetimes.Settheblankfollowingtheprocedureoutlinedintheoperatorsinstructionmanual.Instrumentcalibration/driftcorrection.Loginaminimumof3Standardreplicates.Weighapproximately***gramsofacalibration/driftstandard,enterthemassandstandardidentificationintoappropriatereplicatefields.Note:LECOReferenceMateria***onotrequirepreparation.Seepreparationstatementonthereferencematerialcertificate.上海禹重实业有限公司分析仪服务值得放心。
SamplePreparationSamplingandsamplepreparationisanimportantissuebecausetraditionalmethodsusedtoobtainsamplesforoxygenandnitrogendeterminationaredifferentfromthoserecommendedforhydrogen,especiallywhensamplingmoltenmetal.Themaindifferenceinsteelsamplingproceduresforoxygen/nitrogenandhydrogenisduetothemobilityofhydrogen.Specialprecautionsmustbeusedwhensamplingforhydrogen.Frommoltensteelandiron,asamplemustbequicklyquenchedincoldwaterandchilledinarefrigerantsuchasliquefiednitrogenoramixtureofacetoneandsolidcarbondioxideinordertoreducelossesofhydrogenfromdiffusion.Lossesofoxygenandnitrogenfromdiffusionarenotaproblem.Asamplethatistakenforhydrogenandchilledinarefrigerantcanalsobeusedforoxygenandnitrogendetermination.However,asamplethatistypicallytakenforoxygenand/ornitrogendeterminationisnotsuitableforhydrogendeterminationduetohydrogenloss(diffusion).Surfacecontaminationmustberemovedbyfilingorlightgrinding,usingcarenottooverheatthesample.上海禹重实业有限公司为您提供分析仪,有需求可以来电咨询!金华力可LECO氧氮氢分析仪多少钱
上海禹重实业有限公司致力于提供分析仪,有想法的可以来电咨询!淮安LECO分析仪
InstrumentHighlightsandFeaturesOptionalFeaturesOptionalboom-mountedtouch-screeninterfacepackage(M)promotesanergonomicworkspaceOptionalPerformancePackage(P)addsathree-stagecarriergaspurificationsystem,andadual-loopgasdosemoduleOptionalDualCoolingPackage(D)addsanintegratedliquid-to-airradiatorwithdualcoolingfans.ThisDCoptiongivestheuserthechoiceofliquid-to-liquidcooling,liquid-to-aircooling,oracombinationofbothOptionalintegratedautocleaner(H)automaticallycleanstheupperelectrodeandlowerelectrodetipOptional20-sampleshuttleloaderavailable淮安LECO分析仪
上海禹重实业有限公司在光谱仪,色谱仪,质谱仪,样品前处理一直在同行业中处于较强地位,无论是产品还是服务,其高水平的能力始终贯穿于其中。公司始建于2013-10-22,在全国各个地区建立了良好的商贸渠道和技术协作关系。禹重科技以光谱仪,色谱仪,质谱仪,样品前处理为主业,服务于仪器仪表等领域,为全国客户提供先进光谱仪,色谱仪,质谱仪,样品前处理。禹重科技将以精良的技术、优异的产品性能和完善的售后服务,满足国内外广大客户的需求。
SamplePreparationSamplingandsamplepreparationofref
【详情】InstrumentHighlightsandFeaturesOptionalFeaturesOpt
【详情】力可OHN736&836系列仪器采用惰性熔融法,提供各种无机材料、钢铁、有色金属、硬质合金陶瓷材料中...
【详情】ONH836氧氮氢分析仪高频燃烧红外检测技分析无机材料中的碳、硫含量。采用惰性气体保护熔融法,提供各...
【详情】氧氮氢分析仪的常见故障及解决方法供电正常、通讯正常,点击确认键后分析仪不工作。这是没有水流,炉子温度...
【详情】Procedure-SolidSamples:--Instrumentcalibration/dri...
【详情】