氧氮氢分析仪是快速、准确分析氧、氮、氢元素的、高性能仪器,整机采用模块化、一体化设计,即主机由可靠的脉冲电极炉、高灵敏高精度的检测系统、布局合理和气密性好的气路系统、可靠耐用的电源系统、稳定的电路系统、高校节能的水循环散热系统等六个**的硬件模块单元组成。氧氮氢分析仪的测量原理:测量范围非常。分析样品时,样品被称重后放到样品端口中,然后用载气进行冲洗,防止大气(含氧气和氮气)进入到炉子系统中。石墨坩埚在脉冲炉中脱气,以尽量减少自带的污染。经过稳定阶段后样品落入坩埚中并熔融。样品中的氧与石墨坩埚中的碳反应生成一氧化碳。氮和氢以单质的形式释放。载气和样品气体通过粉尘过滤网后再进入到氧化铜催化炉中,将一氧化碳氧化成二氧化碳。二氧化碳进入到红外池中用于测定氧含量,被测后的气体导入化学试剂管,这时二氧化碳和水被化学试剂除去,氮元素通过热导检测池含量被测定。测量氢时,载气换为氮气,样品气体通过舒茨试剂而不是氧化铜催化剂。测氧和氮时也可采用更廉价的氩气作为载气。上海禹重实业有限公司是一家专业提供分析仪的公司,有想法可以来我司咨询!常州力可LECO分析仪优惠价格
SamplePreparationTypically,titaniumandzirconiumsamplesarechemicallyetchedtoremovesurfacecontaminationwhenoxygenandnitrogenaredetermined.However,etchingcanintroducehydrogenintothesample.ASTMmethodE1409"DeterminationofOxygenandNitrogeninTitaniumandTitaniumAlloysbytheInertGasFusionTechnique",asupdatedin1996,permitseitheretchingorabrading(filing)ofthetestspecimen.ASTME1447"DeterminationofHydrogeninTitaniumandTitaniumAlloysbytheInertGasFusionThermalConductivity/InfraredDetectionMethod"permitssurfacepreparationbyabrading(ifnecessarytoremovecontamination).DifferencesinsamplepreparationpresentsomewhatofadilemmaregardingsimultaneousdeterminationofO,N,andHintitanium.However,abradingsampleswithafiletoremovesurfacecontaminationwillyieldaccurateO,N,andHresults.TheONH836utilizesahigh-powerelectrodefurnacetoquicklyandefficientlyreleasethetargetgasesfromwithinthesample,whichallowsforaveryrapidsimultaneousdeterminationofoxygen,nitrogen,andhydrogen.常州力可LECO分析仪优惠价格分析仪,就选上海禹重实业有限公司,让您满意,欢迎您的来电!
Procedure–Powder/ChipSamplesInstrumentcalibration/driftcorrection.Calibrate/driftfollowingtheprocedureoutlinedintheoperatorsinstructionmanual.AnalyzeSamples.LoginSamplewiththeappropriatenumberofreps.Weighapproximately***gramsofappropriatelypreparedsampleintoa***NickelCapsule,entermassandsampleidentificationintoappropriaterepfields.Ifapplicable,placethenickelcapsuleintheappropriateautoloaderposition.Repeatsteps3cthrough3iforsampleanalysis.
力可ONH836氧氮氢分析仪特征稳固的炉头试样加载结构试样加载过程中完全密闭,消除大气的中可能带来的杂质的污染;简化日常分析所需的炉头进样部分机械维护工作。可选的自动功能上下电极自动清扫装置;20位试样及坩埚自动进样装置。附加功能及优点可选六轴可旋转触摸屏幕,增强了操作的工效和直观性;可选具有压力补偿和温度控制性能的标气检测气路;新型气路管道减少气路连接阀,使得漏气,断路故障更少;配置SmartLineRemote远程诊断功能。上海禹重实业有限公司分析仪值得用户放心。
SamplePreparationSamplingandsamplepreparationisanimportantissuebecausetraditionalmethodsusedtoobtainsamplesforoxygenandnitrogendeterminationaredifferentfromthoserecommendedforhydrogen,especiallywhensamplingmoltenmetal.Themaindifferenceinsteelsamplingproceduresforoxygen/nitrogenandhydrogenisduetothemobilityofhydrogen.Specialprecautionsmustbeusedwhensamplingforhydrogen.Frommoltensteelandiron,asamplemustbequicklyquenchedincoldwaterandchilledinarefrigerantsuchasliquefiednitrogenoramixtureofacetoneandsolidcarbondioxideinordertoreducelossesofhydrogenfromdiffusion.Lossesofoxygenandnitrogenfromdiffusionarenotaproblem.Asamplethatistakenforhydrogenandchilledinarefrigerantcanalsobeusedforoxygenandnitrogendetermination.However,asamplethatistypicallytakenforoxygenand/ornitrogendeterminationisnotsuitableforhydrogendeterminationduetohydrogenloss(diffusion).Surfacecontaminationmustberemovedbyfilingorlightgrinding,usingcarenottooverheatthesample.上海禹重实业有限公司为您提供分析仪,期待为您服务!常州氧氮氢分析仪优惠价格
上海禹重实业有限公司为您提供分析仪,欢迎您的来电!常州力可LECO分析仪优惠价格
Procedure-SolidSamplesPresstheAnalyzebuttonontheinstrumentscreenagain,theloadingheadslide-blockwillcloseandthelowerelectrodewillopen.Cleantheupperandlowerelectrodemanually,or,ifapplicable,removethecrucibleandpresstheanalyzebuttontocleanwiththeautomaticcleanerAddapproximately0.05gof***GraphitePowdertoa***GraphiteCrucible.Firmlyplacethecrucibleonthelowerelectrodetiporappropriateautoloaderposition.PresstheAnalyzebuttonontheinstrumentscreen,thelowerelectrodewillcloseandtheanalysissequencewillstartandendautomatically常州力可LECO分析仪优惠价格
上海禹重实业有限公司主营品牌有赛默飞世尔,发展规模团队不断壮大,该公司服务型的公司。是一家有限责任公司(自然)企业,随着市场的发展和生产的需求,与多家企业合作研究,在原有产品的基础上经过不断改进,追求新型,在强化内部管理,完善结构调整的同时,良好的质量、合理的价格、完善的服务,在业界受到宽泛好评。公司拥有专业的技术团队,具有光谱仪,色谱仪,质谱仪,样品前处理等多项业务。禹重科技以创造***产品及服务的理念,打造高指标的服务,引导行业的发展。
SamplePreparationSamplingandsamplepreparationofref
【详情】InstrumentHighlightsandFeaturesOptionalFeaturesOpt
【详情】力可OHN736&836系列仪器采用惰性熔融法,提供各种无机材料、钢铁、有色金属、硬质合金陶瓷材料中...
【详情】ONH836氧氮氢分析仪高频燃烧红外检测技分析无机材料中的碳、硫含量。采用惰性气体保护熔融法,提供各...
【详情】氧氮氢分析仪的常见故障及解决方法供电正常、通讯正常,点击确认键后分析仪不工作。这是没有水流,炉子温度...
【详情】Procedure-SolidSamples:--Instrumentcalibration/dri...
【详情】